Preparation and characterization of lead zirconate ceramics from high-energy ball milled powder

L. B. Kong; J. Ma; W. Zhu; O. K. Tan

doi:10.1016/S0167-577X(00)00350-5

Preparation and characterization of lead zirconate ceramics from high-energy ball milled powder

L. B. Kong^*, J. Ma, W. Zhu, O. K. Tan

^*Corresponding author for this work

Nanyang Technological University

Research output: Contribution to journal › Article › peer-review

18 Citations (Scopus)

Abstract

Lead zirconate (PbZrO₃ or PZ) powder was successfully synthesized by a high-energy ball milling process using oxides as starting materials. The milled powders were characterized by XRD, SEM and particle size analysis. Perovskite PZ phase is predominant in the milled powder with an average particle size of about 20 nm. The sintering behavior of the milled powder was investigated by a dilatometer, showing a maximum densification occurred at about 950°C. PZ ceramics were obtained by sintering the milled powder at different temperatures. The microstructure, grain growth, density and dielectric property of the PZ ceramics as a function of sintering temperature were investigated and discussed.

Original language	English
Pages (from-to)	96-101
Number of pages	6
Journal	Materials Letters
Volume	49
Issue number	2
DOIs	https://doi.org/10.1016/S0167-577X(00)00350-5
Publication status	Published - Jun 2001
Externally published	Yes

ASJC Scopus Subject Areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Keywords

Dielectric properties
High-energy ball milled powder
Lead zirconate ceramics
PbZrO

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10.1016/S0167-577X(00)00350-5

Cite this

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title = "Preparation and characterization of lead zirconate ceramics from high-energy ball milled powder",

abstract = "Lead zirconate (PbZrO3 or PZ) powder was successfully synthesized by a high-energy ball milling process using oxides as starting materials. The milled powders were characterized by XRD, SEM and particle size analysis. Perovskite PZ phase is predominant in the milled powder with an average particle size of about 20 nm. The sintering behavior of the milled powder was investigated by a dilatometer, showing a maximum densification occurred at about 950°C. PZ ceramics were obtained by sintering the milled powder at different temperatures. The microstructure, grain growth, density and dielectric property of the PZ ceramics as a function of sintering temperature were investigated and discussed.",

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year = "2001",

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language = "English",

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pages = "96--101",

journal = "Materials Letters",

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T1 - Preparation and characterization of lead zirconate ceramics from high-energy ball milled powder

AU - Kong, L. B.

AU - Ma, J.

AU - Zhu, W.

AU - Tan, O. K.

PY - 2001/6

Y1 - 2001/6

N2 - Lead zirconate (PbZrO3 or PZ) powder was successfully synthesized by a high-energy ball milling process using oxides as starting materials. The milled powders were characterized by XRD, SEM and particle size analysis. Perovskite PZ phase is predominant in the milled powder with an average particle size of about 20 nm. The sintering behavior of the milled powder was investigated by a dilatometer, showing a maximum densification occurred at about 950°C. PZ ceramics were obtained by sintering the milled powder at different temperatures. The microstructure, grain growth, density and dielectric property of the PZ ceramics as a function of sintering temperature were investigated and discussed.

AB - Lead zirconate (PbZrO3 or PZ) powder was successfully synthesized by a high-energy ball milling process using oxides as starting materials. The milled powders were characterized by XRD, SEM and particle size analysis. Perovskite PZ phase is predominant in the milled powder with an average particle size of about 20 nm. The sintering behavior of the milled powder was investigated by a dilatometer, showing a maximum densification occurred at about 950°C. PZ ceramics were obtained by sintering the milled powder at different temperatures. The microstructure, grain growth, density and dielectric property of the PZ ceramics as a function of sintering temperature were investigated and discussed.

KW - Dielectric properties

KW - High-energy ball milled powder

KW - Lead zirconate ceramics

KW - PbZrO

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JO - Materials Letters

JF - Materials Letters

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ER -

Preparation and characterization of lead zirconate ceramics from high-energy ball milled powder

Abstract

ASJC Scopus Subject Areas

Keywords

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