Rapid formation of lead magnesium niobate-based ferroelectric ceramics via a high-energy ball milling process

L. B. Kong; J. Ma; W. Zhu; O. K. Tan

doi:10.1016/S0025-5408(01)00823-6

Rapid formation of lead magnesium niobate-based ferroelectric ceramics via a high-energy ball milling process

L. B. Kong^*, J. Ma, W. Zhu, O. K. Tan

^*Corresponding author for this work

Nanyang Technological University

Research output: Contribution to journal › Article › peer-review

23 Citations (Scopus)

Abstract

Pyrochlore-free nano-sized 0.90Pb(Mg_1/3Nb_2/3)O₃(PMN)-0.10PbTiO₃ (PT) and 0.65PMN-0.35PT powders were synthesized from oxides via a high-energy ball milling process. Single perovskite phase PMN-PT were readily formed from the oxide mixture after milling for only 2 h. The grain size calculated from X-ray diffraction (XRD) patterns of all samples is about 20 nm, which is in agreement with the observation from scanning electron microscopy (SEM) (20-50 nm). PMN-PT ceramics were obtained by sintering the milled powders at temperature from 1000 to 1100 °C for 2 h. The dielectric, ferroelectric properties of the PMN-PT ceramics derived from the synthesized powders were comparable with the reported results in the literature.

Original language	English
Pages (from-to)	459-465
Number of pages	7
Journal	Materials Research Bulletin
Volume	37
Issue number	3
DOIs	https://doi.org/10.1016/S0025-5408(01)00823-6
Publication status	Published - Mar 1 2002
Externally published	Yes

ASJC Scopus Subject Areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Keywords

A. Ceramics
D. Ferroelectricity

Access to Document

10.1016/S0025-5408(01)00823-6

Cite this

@article{32905113bba04ce4ad0c1de2c907fd9e,

title = "Rapid formation of lead magnesium niobate-based ferroelectric ceramics via a high-energy ball milling process",

abstract = "Pyrochlore-free nano-sized 0.90Pb(Mg1/3Nb2/3)O3(PMN)-0.10PbTiO3 (PT) and 0.65PMN-0.35PT powders were synthesized from oxides via a high-energy ball milling process. Single perovskite phase PMN-PT were readily formed from the oxide mixture after milling for only 2 h. The grain size calculated from X-ray diffraction (XRD) patterns of all samples is about 20 nm, which is in agreement with the observation from scanning electron microscopy (SEM) (20-50 nm). PMN-PT ceramics were obtained by sintering the milled powders at temperature from 1000 to 1100 °C for 2 h. The dielectric, ferroelectric properties of the PMN-PT ceramics derived from the synthesized powders were comparable with the reported results in the literature.",

keywords = "A. Ceramics, D. Ferroelectricity",

author = "Kong, {L. B.} and J. Ma and W. Zhu and Tan, {O. K.}",

year = "2002",

month = mar,

day = "1",

doi = "10.1016/S0025-5408(01)00823-6",

language = "English",

volume = "37",

pages = "459--465",

journal = "Materials Research Bulletin",

issn = "0025-5408",

publisher = "Elsevier Limited",

number = "3",

}

TY - JOUR

T1 - Rapid formation of lead magnesium niobate-based ferroelectric ceramics via a high-energy ball milling process

AU - Kong, L. B.

AU - Ma, J.

AU - Zhu, W.

AU - Tan, O. K.

PY - 2002/3/1

Y1 - 2002/3/1

N2 - Pyrochlore-free nano-sized 0.90Pb(Mg1/3Nb2/3)O3(PMN)-0.10PbTiO3 (PT) and 0.65PMN-0.35PT powders were synthesized from oxides via a high-energy ball milling process. Single perovskite phase PMN-PT were readily formed from the oxide mixture after milling for only 2 h. The grain size calculated from X-ray diffraction (XRD) patterns of all samples is about 20 nm, which is in agreement with the observation from scanning electron microscopy (SEM) (20-50 nm). PMN-PT ceramics were obtained by sintering the milled powders at temperature from 1000 to 1100 °C for 2 h. The dielectric, ferroelectric properties of the PMN-PT ceramics derived from the synthesized powders were comparable with the reported results in the literature.

AB - Pyrochlore-free nano-sized 0.90Pb(Mg1/3Nb2/3)O3(PMN)-0.10PbTiO3 (PT) and 0.65PMN-0.35PT powders were synthesized from oxides via a high-energy ball milling process. Single perovskite phase PMN-PT were readily formed from the oxide mixture after milling for only 2 h. The grain size calculated from X-ray diffraction (XRD) patterns of all samples is about 20 nm, which is in agreement with the observation from scanning electron microscopy (SEM) (20-50 nm). PMN-PT ceramics were obtained by sintering the milled powders at temperature from 1000 to 1100 °C for 2 h. The dielectric, ferroelectric properties of the PMN-PT ceramics derived from the synthesized powders were comparable with the reported results in the literature.

KW - A. Ceramics

KW - D. Ferroelectricity

UR - http://www.scopus.com/inward/record.url?scp=0036497185&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0036497185&partnerID=8YFLogxK

U2 - 10.1016/S0025-5408(01)00823-6

DO - 10.1016/S0025-5408(01)00823-6

M3 - Article

AN - SCOPUS:0036497185

SN - 0025-5408

VL - 37

SP - 459

EP - 465

JO - Materials Research Bulletin

JF - Materials Research Bulletin

IS - 3

ER -

Rapid formation of lead magnesium niobate-based ferroelectric ceramics via a high-energy ball milling process

Abstract

ASJC Scopus Subject Areas

Keywords

Access to Document

Other files and links

Fingerprint

Cite this