Spark plasma sintering of silver nanopowder

H. B. Ng, C. Shearwood, T. J. White, L. G. Yu, K. A. Khor

Research output: Chapter in Book/Report/Conference proceedingConference contribution

2 Citations (Scopus)

Abstract

The spark plasma sintering behaviour of silver nanopowder prepared by the electro-explosion method was investigated. Consolidation was carried out from 50°C to 800°C for 5 mins at 34 MPa with differential scanning calorimetry indicating a sintering onset temperature as low as 160°C and an activation energy of 86±1 kJ/mol. Near full density resulted from treatment at 300°C, and at higher temperatures a normal Hall-Petch relation is obeyed. The enhancement of Vicker's hardness to 1000MPa for materials sintered at 300°C is three times greater than for silver annealed in a conventional way. While polysynthetic twinning contributes to superior hardness, the primary cause is the sub-micron grain size.

Original languageEnglish
Title of host publicationBioMEMS and Nanotechnology III
DOIs
Publication statusPublished - 2008
Externally publishedYes
EventBioMEMS and Nanotechnology III - Canberra, ACT, Australia
Duration: Dec 5 2007Dec 7 2007

Publication series

NameProgress in Biomedical Optics and Imaging - Proceedings of SPIE
Volume6799
ISSN (Print)1605-7422

Conference

ConferenceBioMEMS and Nanotechnology III
Country/TerritoryAustralia
CityCanberra, ACT
Period12/5/0712/7/07

ASJC Scopus Subject Areas

  • Electronic, Optical and Magnetic Materials
  • Atomic and Molecular Physics, and Optics
  • Biomaterials
  • Radiology Nuclear Medicine and imaging

Keywords

  • Grain growth
  • Hardness
  • Nanocrystalline materials
  • Nanopowder
  • Silver
  • Sintering
  • Twinning

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