Surface characterization of plasma sprayed hydroxyapatite coatings

Limin Sun*, Christopher C. Berndt, A. Kucuk, R. S. Lima, K. A. Khor

*Corresponding author for this work

Research output: Contribution to journalConference articlepeer-review

1 Citation (Scopus)

Abstract

Plasma sprayed hydroxyapatite (HA) coatings have been widely used for dental and orthopedic applications for fast fixation between the implant and the human anatomy. In this study, the HA coatings were atmospherically plasma sprayed (APS) using different spray power and stand-off distance (SOD), and the coating surfaces were characterized using various methods. X-ray diffraction (XRD) revealed the presence of crystalline HA, amorphous calcium phosphate (ACP) and some other crystalline phases including tricalcium phosphate (α-TCP and β-TCP), tetracalcium phosphate (TTCP) and calcium oxide (CaO). Fourier transform infrared (FTIR) spectroscopy showed that both OH and PO43- bands of HA changed after spraying and the HA phase identified by XRD was actually the solid solution of oxyapatite (OAp) in HA, i.e., oxyhydroxyapatite (OHA). The phase composition of the HA coatings varied with respect to the spray power and SOD. The surface morphology and roughness were analyzed via scanning electron microscopy (SEM) and profilometry respectively, and the results related to the phase composition.

Original languageEnglish
Pages (from-to)251-258
Number of pages8
JournalCeramic Engineering and Science Proceedings
Volume21
Issue number4
Publication statusPublished - 2000
Externally publishedYes
Event24th Annual Conference on Composites, Advanced Ceramics, Materials,and Structures:B - Cocoa Beach, FL, USA
Duration: Jan 23 2000Jan 28 2000

ASJC Scopus Subject Areas

  • Ceramics and Composites
  • Materials Chemistry

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