Thermal curing of hydrogen silsesquioxane

Y. K. Siew*, G. Sarkar, X. Hu, J. Hui, A. See, C. T. Chua

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

66 Citations (Scopus)

Abstract

Thin film characterization techniques such as Fourier transform infrared spectroscopy and ellipsometry and thermal analysis techniques such as differential scanning calorimetry, thermogravimetric analysis, and dielectric thermal analysis were used to monitor the thermal curing of hydrogen silsesquioxane. This study gives evidence which support the notion that the redistribution of Si-O and Si-H bonds is the reaction mechanism responsible for the chemical changes induced by heating. Curing of hydrogen silsesquioxane is found to be accompanied by weight loss, dimension change, and change in dielectric properties. A three-stage curing process has been postulated based on the data collected.

Original languageEnglish
Pages (from-to)335-339
Number of pages5
JournalJournal of the Electrochemical Society
Volume147
Issue number1
DOIs
Publication statusPublished - Jan 2000
Externally publishedYes

ASJC Scopus Subject Areas

  • Electronic, Optical and Magnetic Materials
  • Renewable Energy, Sustainability and the Environment
  • Surfaces, Coatings and Films
  • Electrochemistry
  • Materials Chemistry

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